Morpholin-4-ium morpholine-4-carbo­dithio­ate

نویسندگان

  • Ana C. Mafud
  • Edgar A. Sanches
  • Maria Teresa Gambardella
چکیده

The title compound, C(4)H(10)NO(+)·C(5)H(8)NOS(2) (-), is built up of a morpholinium cation and a dithio-carbamate anion. In the crystal, two structurally independent formula units are linked via N-H⋯S hydrogen bonds, forming an inversion dimer, with graph-set motif R(4) (4)(12).

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4-[(2′-Cyano­biphen­yl-4-yl)meth­yl]morpholin-4-ium tetra­fluoridoborate

In the crystal structure of the title compound, C(18)H(19)N(2)O(+)·BF(4) (-), bifurcated N-H⋯(F,F) hydrogen bonds link the protonated 4'-morpholine-methyl-biphenyl-2-carbonitrile cations and slightly distorted tetra-fluoro-borate anions. π-π inter-actions [centroid-centroid distance = 3.805 (3) Å] help to consolidate the packing. The dihedral angle between the benzene rings in the cation is 57....

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Morpholin-4-ium hydrogen l-tartrate monohydrate

In the title compound, C(4)H(10)NO(+)·C(4)H(5)O(6) (-)·H(2)O, the morpholine ring adopts a chair conformation. In the crystal, the tartrate anions are linked via O-H⋯O hydrogen bonds, forming chains propagating along [101]. These chains are linked via N-H⋯O and O-H⋯O hydrogen bonds, involving the morpholinium cation and the water molecule, forming a three-dimensional network.

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Dimethyl­ammonium bis­(4-methyl­morpholin-4-ium) tetra­chloridozincate

The title compound, (C(2)H(8)N)(C(5)H(12)NO)[ZnCl(4)], was synthesized by hydro-thermal reaction of ZnCl(2) with 4-methyl-morpholine in a dimethyl-formamide solution. The asymmetric unit is composed of half a [ZnCl(4)](2-) anion, half a 4-methyl-morpholin-4-ium cation and half a dimethyl-ammonium cation, all located on mirror planes parallel to ac. All the amine H atoms are involved in inter-mo...

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4-[(2′-Cyano­biphenyl-4-yl)methyl]­morpholin-4-ium nitrate

The title ion pair, C(18)H(19)N(2)O(+)·NO(3) (-), features an N-H⋯O hydrogen bond linking the cation to the anion. The morpholine portion adopts a chair conformation; the aromatic rings of the biphenyl-ene portion are twisted [torsion angles for the four atoms involving the ar-yl-aryl bond = 35.1 (2)-40.4 (2)°].

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Tetra­kis{4-[(2H-tetra­zol-5-yl)meth­yl]morpholin-4-ium} dodeca­tungstosilicate hexa­hydrate

The crystal structure of the title compound, (C(6)H(12)N(5)O)(4)[W(12)(SiO(4))O(36)]·6H(2)O, consists of an α-Keggin-type [W(12)(SiO(4))O(36)](4-) polyoxidoanion, four [(2H-tetra-zol-5-yl)meth-yl]morpholinium cations and six uncoordinated water mol-ecules. In the cations, the morpholine rings display chair conformations. Extensive N-H⋯O, N-H⋯N, O-H⋯O and O-H⋯N hydrogen bonds are present in the ...

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عنوان ژورنال:

دوره 67  شماره 

صفحات  -

تاریخ انتشار 2011